4,4',4''-phosphinetriyltris[N,N-dimethylaniline]
Basic Information
- CAS No.:1104-21-8
Physical properties
Product Description
Buy cost-effective 99% pure 4,4',4''-phosphinetriyltris[N,N-dimethylaniline] 1104-21-8 now
- Molecular Formula:C24H30 N3 P
- Molecular Weight:391.496
- Boiling Point:518.7°Cat760mmHg
- Flash Point:267.5°C
- PSA：23.31000
- Density:g/cm3
- LogP:3.64280
1104-21-8 Relevant articles
Synthesis, Structure, and Reactivities of Iminosulfane- and Phosphane-Stabilized Carbones Exhibiting Four-Electron Donor Ability
Morosaki, Tomohito,Wang, Wei-Wei,Nagase, Shigeru,Fujii, Takayoshi
, p. 15405 - 15411 (2015)
Iminosulfane(phosphane)carbon(0) derivat...
PHOSPHORYLATION OF AROMATIC COMPOUNDS HAVING ELECTRON-DONOR SUBSTITUENTS WITH PHOSPHOROUS TRIBROMIDE
Tolmachiev, A. A.,Ivonin, S. P.,Kharchenko, A. V.,Kozlov, E. S.
, p. 1057 - 1058 (2007/10/02)
-
Syntheses and Spectroscopic Investigations of Substituted cis- and trans-Dichlorobis(triphenylphospane)platinum(II) Compounds
Brune, Hans Albert,Falck, Manfred,Hemmer, Reinhard,Schmidtberg, Guenter,Alt, Helmut G.
, p. 2791 - 2802 (2007/10/02)
Compounds of the type cis- and trans-dic...
1104-21-8 Process route
-
-
121-69-7,77733-26-7
N,N-dimethyl-aniline
-
-
10025-87-3,12599-09-6,63736-95-8,39380-77-3
trichlorophosphate
-
-
7439-52-3
bis(p-(dimethylamino)phenyl)phosphonic acid
-
-
101-61-1
4,4'-methylene-bis(N,N-dimethylaniline)
-
-
1104-21-8
tris(p-dimethylaminophenyl)phosphine
| Conditions | Yield |
|---|---|
|
at 130 ℃;
nachfolgenden Behandeln mit verd.Natronlauge;
|
-
-
586-77-6
4-bromo-N,N-dimethylaniline
-
-
1104-21-8
tris(p-dimethylaminophenyl)phosphine
| Conditions | Yield |
|---|---|
|
4-bromo-N,N-dimethylaniline;
With
magnesium; lithium chloride;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
phosphorus tribromide;
at 0 - 20 ℃;
for 0.333333h;
Inert atmosphere;
|
80% |
|
With
magnesium; phosphorus trichloride;
Yield given. Multistep reaction;
1) THF, 2) THF, 0 deg C;
|
1104-21-8 Upstream products
-
29972-74-5
(4-dimethylamino-phenyl)-phosphonous acid dichloride
-
13190-50-6
4-dimethylaminophenyllithium
-
121-69-7
N,N-dimethyl-aniline
-
586-77-6
4-bromo-N,N-dimethylaniline
1104-21-8 Downstream products
-
60271-45-6
[4-(2-benzothiazol-2-yl-vinyl)-benzyl]-tris-(4-dimethylamino-phenyl)-phosphonium; bromide
-
24764-39-4
Tris-(4-dimethylamino-phenyl)-<2,7-dibrom-fluorenyliden-(9)>-phosphoran
-
22883-69-8
Benzyl-tris-(4-dimethylamino-phenyl)-phosphonium; bromide
-
39135-06-3
N-phenyl-P,P,P-tris